Pdf oxidation resistance and wetting behavior of mgoc. Porosity was evaluated by using the settime equilibrium 10 s mode between the pressure limits of 0. The autopore iv software allows you to enter the precise. Autopore iv 9500, from micromeritics, and the solid density, determined by helium pycnometry at 35 c in an accupyc 30 from micromeritics. Related content from micromeritics instrument corporation. The raman spectra were acquired on a jobinyvon labram hr 800 microraman system. This is called mercury porosimetry, or often, mercury intrusion. Implication and evaluation of micromeritics in formulation by. Pdf using xray computed tomography in pore structure. Abele1,2 1 institute of production management, technology and machine tools ptw, technische universitat darmstadt, germany.
Autopore iv 9500 has not been rated by our users yet. As particle size decreases v, area increases 20140223 3 faculty of pharmacy, omer almukhtar university, tobruk, libya. Autopore iv 9500 is a shareware software in the category miscellaneous developed by autopore iv 9500. Speciicaions autopore iv 9500 series low pressure measurement 0 to 50 psia 345 kpa pore diameter range 360 to 3. Autopore iv series 9500 and 9510 mercury porosimetery.
Autopore v series mercury porosimeters pharmaceutical online. Micromeritics autopore iv 9500 series characterizes a materials porosity by. Micromeritics also offers a large selection of penetrometer bulbs, volumes, stems, and closures designed to fit most sample forms. Micromeritics autopore iv 9500 particle technology labs. Mercury intrusion porosimetry mip using micromeritics autopore iv 9500, micromeritics instrument corp. The porosity and pore size distribution were analyzed by using mercury porosimetry autopore iv 9500, micromeritics, shang hai, china. The open porosity and pore size were measured using a mercury porosimetry autopore iv 9500, micromeritics, usa. Micromeritics autopore iv 9500 series characterizes a materials porosity by applying various levels of pressure to a sample immersed in mercury. The autopore iv 9500 series of mercury porosimeters from micromeritics enable the user to calculate numerous sample properties. Both models can reach a maximum pressure of 33,000 psia and measure pore diameters ranging from 360. The autopore v series mercury porosimeters can determine a broader pore size distribution more quickly and accurately than other methods. Introduction the science and technology of small particles was given by the name micromeritics by dalla valle micromeritics is the science and technology of small particles. This document will provide a detailed operation procedure of the micromeritics autopore iv po.
Dec 30, 2017 micromeritics autopore iv 9500 series characterizes a materials porosity by applying various levels of pressure to a sample immersed in mercury. Analysis of particle size distribution the particle size distribution and the average diameter were measured by laser diffractometry using mastersizer 2000e. Changes in physicochemical and biological properties of. Autopore iv 9500, micromeritics, norcross, ga, usa.
Fabrication of porous al2o3 ceramics with submicronsized. The apparent density of the biochar evaluated in this work is large compared to other gac developed from the same precursor by co 2 activation due to the narrower pore size distribution of the biochar. These include pore size distributions, total pore volume, total pore surface area, median pore diameter and sample densities bulk and skeletal. Micromeritics autopore v series mercury intrusion porosimeters are available in two models to suit the needs of research and quality assurance laboratories. Experimental and simulation study of adsorption in. Autopore iv 9500 series measures sample porosity laboratory. Autopore iv 9500 nonwetting fluid mercury intrusion device, by pressure, for pore size distribution determining in solid porous sample.
The mercury porosimetry analysis technique is based on the intrusion of mercury into a porous structure under stringently controlled pressures. Experiments were conducted in accordance with the protocol given in the autopore iv 9500 operators manual. Autopore iv 9500, micromeritics, norcross, ga, usa, in the pressure range of 0. Microstructure and diffraction patterns of the fragment samples separated from coating layer were analyzed by 200 kv fetem field emission transmission electron microscope, tecnai g2 f20. Model 9505 from atmospheric pressure to 33,000 psia 228 mpa model 9520 from atmospheric pressure to 60,000 psia 414 mpa pore diameter. Material characterization the archimedes method was used to measure the bulk densities of the porous. In order to measure porosity in the range from 1 mm down to 2 nm, a micromeritics autopore iv 9500 porosimeter micromeritics instrument corporation, norcross ga, us was used. Finally, pore structure was evaluated by mercury intrusion porosimetry.
Click here to download the autopore iv series porosimeters brochure in pdf. The aim of the present study was to investigate asiii oxidation and adsorption on the surface of hybrid anion exchangers containing cuiifeiii b. Three independently measured density values are average out and reported as the density of the sintered sample. The bulk density was measured by the archimedes method in water medium, as shown in equation 1 14. Mercury intrusion porosimetry mip is a powerful technique utilized for the evaluation of porosity, pore size distribution, and pore volume among others to characterize a wide variety of solid and powder materials. It was initially added to our database on 07082008. Mercury intrusion pressure is raised automatically, up to 220 mpa, and intruded volume into sample is related with porosity determination. The autopore iv 9500 has two low pressure ports and one high pressure port. Speciicaions autopore iv 9500 series micromeritics. The autopore iv uses pressurized mercury to measure the pore sizes in materials. An mip instrument autopore iv 9500, micromeritics was used to measure the pore size distributions. Mercury intrusion porosimeter scientific and technical. The 9505 has four low and two highpressure chambers. Autopore iv 9500 runs on the following operating systems.
It is the science and technology of small particles. Fabrication of icetemplated tubes by rotational freezing. Autopore iv series porosimeters pharmaceutical online. Passive human body cooling a wearable polyethylenepolyamide. Besides offering speed, accuracy, and a wide measurement range, mercury porosimetry permits you to calculate numerous sample properties. Mercury intrusion porosimetry particle technology labs. The autopore iv 9605 series has 4 lowpressure ports and 2 highpressure ports for analysis at up to 33,000psia. Autopore iv 9500 series specifications general low pressure. The pressure applied by the intrusion porosimeter ranged from 0 to 200 mpa in step mode. Bap is found to be much closer to the formation rate of human bones 1,2. The autopore iv series is available in four models to best match the needs of individual quality assurance and research labs. The autopore v series mercury porosimeters can determine a broader pore size distribution. Micromeritics autopore iv 9500 series characterizes a materials. The autopore iv software allows you to enter the precise angle of contact.
Autopore iv series mercury porosimeter 9500 and 9510. The instrument, known as a porosimeter, employs a pressurized chamber to force mercury to intrude into the voids in a porous. Sic conversion coating prepared from silicagraphite reaction. Effects of the molding method and blank size of green body on. Overview micromeritics autopore iv 9500 series characterizes a materials porosity by applying various levels of pressure to a sample immersed in mercury. The pore size distribution of the sic coating was analyzed by mercury intrusion porosimetry autopore iv 9500 micromeritics instrument. Tunable and weakly negative permittivity in carbonsilicon.
The latest version of autopore iv 9500 is currently unknown. All the experiments were conducted with a universal testing machine shimadzu model agsx, kyoto. The autopore iv 9500 has two low and one highpressure chamber. Fabrication steps of porous al2o3 ceramics by gelcasting, a al2o3 suspension. The pressure required to intrude mercury into the samples pores is inversely proportional to the size of the pores. Micromeritics, auto pore iii, mercury intrusion porosimeter. For determining the exact contact angle, micromeritics offers. Mercury intrusion porosimetry mip is a powerful technique utilized for the evaluation of porosity, pore size. Synthesis of macroporous polystyrenedivinyl benzene. Micromeritics autopore iv porosimeters 9500 series. Sample data outputs from analyses including bet specific surface area. The autopore iv can accurately collect the data that provide the basis for.
This measurement is based on the nonwetting behavior of mercury to most materials and takes advantage of the relationship of pore size and the intrusion pressure. Micromeritics mercury porosimeter autopore iv created date. Mechanical properties of icetemplated tubes were characterized by two different tests. The bulk density was measured by the archimedes method in. This instrument also features enhanced safety features and offers new data reduction and reporting choices that provide more information about pore geometry and the fluid transport characteristics of your material. High sulfate attack resistance of reinforced concrete. Agilent e4991a precision impedance analyzer combined with 16453a dielectric test. Our latest offering, the autopore iv series of mercury porosimeters, provides the same highquality analysis data as expected from other micromeritics products and, in addition, comes with enhanced data reduction and reporting packages, faster pressure ramp rates, a more flexible and controllable vacuum system, and a redesign of both the low. A choice of correction routine for baseline automatic, differential, or manual produces greater.
Other collected fragments were were used for sem tests. Autopore iv 9500 mercury porosimetry micromeritics, usa. The apparent porosity of the specimens was measured by the archimedes method. Hydration development and thermal performance of calcium.